ICP-MS法同时测定钢渣中10种矿质元素
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国家十一·五科技支撑计划课题(2008BADA9B08)资助。


Analysis of 10 mineral elements in slag by ICP-MS
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    摘要:

    建立了钢渣中多种矿质元素的检测方法。钢渣样品经HNO3-HF-HClO4消化,采用电感耦合等离子体质谱(ICP-MS)法检测钢渣中10种矿质元素。该方法的检出限为0.002~6.68 μg·g-1,加标回收率为78.8%~105.7%,相对标准偏差(RSD)为0.68%~8.29%。该方法具有简便、快速、准确等特点,可用于钢渣中矿质元素的分析。

    Abstract:

    Inductive coupled plasma mass spectrometry (ICP-MS) was used to analyze the contents of 10 mineral elements in slag. After digested completely by HNO3-HF-HClO4, these samples were determined using the internal method. The recoveries for spiking samples were 78.8%-105.7%, and the relative standard deviations were 0.68%-8.29%. The range of the detection limits of elements was 0.002-6.68 μg·g-1. The proposed method is simple, rapid and accurate, and could be used to analyze mineral elements in the slag.

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  • 在线发布日期: 2016-12-07